Structural, Optical and Thermal Characterization of Synthesised Heterocyclic Organic Compound
Arpitha Kumari *
Department of Physics Mangalore University, 5742199, India.
Ganesh Sanjeev
Department of Physics, Mangalore University, Mangalagangothri, India.
Boja Poojari
Department of Chemistry, Mangalore University, Mangalagangothri, India.
P. V. Soumya
Department of Chemistry, Mangalore University, Mangalagangothri, India.
*Author to whom correspondence should be addressed.
Abstract
A heterocyclic organic compound of 3-[(2z)-2-methyl-3-(4-nitrophenyl) prop-2-enoyl]-2H-(1-benzopyran-2-one) (MNB) is synthesized using Claisen-Schmidth condensation reaction. Structural characterization and presence of functional groups are carried out using powder X-ray diffractogram and FTIR spectroscopic studies respectively. Thermogravimetric analysis and differential thermal analysis are carried out to determine the melting property and it shows good thermal stability among organic crystal showing result at 166°C. Second Harmonic Generation efficiency study is carried out using Nd: YAG laser, this revealed that titled compound is good for NLO characterization and applicable in optoelectronics. PL wavelength present in visible region conclude that sample shows fluorescence property.
Keywords: Heterocyclic organic compound, powder XRD, Photoluminescence, second harmonic generation.